Instrumental parameters Conditions
Injection volume 1 µL
Injection mode spitless
Injection time 0.5 min
Injector temperature 250 ºC
Capillary column Restek, FAMEWAS ® WCOT fused silica 30m x 0.25 mm x 0.25 µm
Carrier gas Helium
Gas flow 1 mL min-1
Temperature program 120 ºC for 1 min, 30 ºC min-1 up to 160 ºC, 160 ºC for 1 min, 4 ºC min-1 up to 240 ºC, and 240 ºC for 7 min
Total time of temperature program 30.33 min
Detector temperature 260 ºC