Table 1: Selected bond lengths (in Å) and angles (in °) of compound 1.
Cobalt-ligand bonds in Å
Co–OOH
2.091(3) – 2.146(3)
Co–µ3-Obda
1.947(3) – 2.046(3)
Co–µ4-Obda
2.026(3) – 2.162(2)
Co–Nbda
2.199(3) – 2.238(3)
Co–Oib (chelating)
2.108(3) and 2.150(3)
Co–Oib (η1 of µ3-η1:η2 ib–)
2.064(3) and 2.096(3)
Co–Oib (η2 of µ3-η1:η2 ib–)
2.104(3) – 2.466(3)
Co···Co (neighboring)
3.096 – 3.217
Co···Co (longest)
9.606
Co3···Co3´
5.556
Co1-oxo-Co angles in °
Co1–O–Co1´
Co1–O–Co2
Co1–O–Co3
Co1–O–Co3´
Co1–O–Co4´
98.26(11)
95.66(11) and 96.45(11)
97.70(11) and 99.55(11)
97.65(12) and 98.33(11)
95.21(11) and 96.23(10)
Co1–O–Co5´
98.72(10) and 99.36(11)
Symmetry code: (i) −x+1, −y+1, −z+1.